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Stirrers and Hot Plates Selection Guide

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Stirrer Types
  • Compact: Small, colorful units fit in any lab.
  • Specialty: An illuminating stirrer and a modular unit that offers remote immersible mixing.
  • Multiposition: Synchronously stir a number of vessels at the same time. Some models let you stir different vessels at different speeds.
  • Multiposition/Immersible: Immersible sitters can be placed completely underwater for constant temperature operations. Ideal for use in incubators.

Stirrer, Hot Plate, and Hot Plate/Stirrer Types

  • Analog: Here is where you will find the basic hot plates and stirrers that you know you can count on—names like Cimarec®, Corning®, and Vela®.
  • Digital: Digital units will meet your needs for greater accuracy and more features. Find names like Mirak®, Heidolph, Jenway, and Cole-Parmer. Programmable models can be programmed directly from the front panel to control speed, temperature, and time.
  • Multiposition: Synchronously stir a number of vessels at the same time. Some models let you stir and heat different vessels at different speeds and temperatures.
  • Glass Top: Two units which offer quick heat up and a modern, easy-to-clean surface.
  • Large Capacity: Four units—with one that can handle up to 150 liters.
  • Explosion Proof: Class I, Group C and D environments.
  • Heavy Duty: Made to withstand even the toughest environments.

Stir Bars

  • A variety of sizes for any application; PTFE coated for chemical resistance; alnico V magnets for consistent coupling.

Selecting Stirrers and Hot Plates:
Five Important Factors

Accuracy and Stability

Basic analog heating and stirring units are not designed to provide exact control over temperature or stirring speed. However, such units do offer economy, reliability, and ease of use when precise control is not required.

Offering somewhat better heat control are units with demand-type bimetallic thermostats that sense changes in top plate temperature through a mechanical connection to the top plate. Such units simulate closed-loop control and minimize temperature overshoot.

For applications in which the control of temperature and stirring speed is crucial (heat control stability better than ±8°C and stirring speed and control better than ±20 rpm), digital heating and stirring equipment with electronic feedback controls offer the greatest degree of accuracy and stability. A closed-loop PID microprocessor control monitors top plate temperatures and/or stirring speeds and automatically compensates for changes in the system relative to a selected set point.

Although more costly, these precise controls can hold a specific temperature or stirring speed, minimize temperature overshoot and undershoot, accurately monitor top-plate and solution temperatures, and in some advanced models, even program heat ramp settings for reproducible results.

Range and Uniformity

The range of temperatures achievable by your hot plate and the uniformity of temperature across its surface are determined by two factors—top plate composition (ceramic, porcelain, or aluminum) and the type of temperature control.

Primary advantages of the ceramic top plate are that it heats quickly and is highly resistant to corrosion. One of the drawbacks is that it does not offer the same uniformity of temperature across the top plate surface that other top plate materials do. Ceramic tops are also susceptible to thermal shock and should not be used when heating metal vessels or sand baths.

Porcelain top plates offer improved temperature uniformity and good resistance to corrosion. Their surface, however, may flex somewhat near maximum temperatures. Both ceramic and porcelain top plates offer better sample visibility than their aluminum counterparts.

Superior temperature uniformity and stability are the primary advantages of aluminum top plates. Typically, aluminum top plates offer temperature uniformity of ±10°C, depending on the top plate size and operation temperature. They are ideal for larger hot plate surfaces and for applications involving multiple vessels. Although they are generally resistant to physical forces, they are vulnerable to corrosive environments and generally are more difficult to clean.

Volume

Hot plates, stirrers, and stirring hot plates come in many different sizes and configurations—from small, single-vessel units to large-capacity, multi-unit ones. Units designed for synchronous stirring and heating of multiple vessels are available with individual stir controls for as many as nine vessels.

Viscosity

When it comes to magnetic coupling strength, all stirrers are not created equal. The ability of a drive-magnet and stir-bar combination to effectively stir a given solution is a function of several variables such as drive-magnet shape and size, stir-bar shape and size, distance between the stir bar and drive magnet, vessel shape and size, desired stir speed, and your solution's viscosity.

Given normal conditions, most stirrers will perform adequately at stirring seeds between 100 rpm and 1000 rpm. Stirring more viscous solutions, however, requires a unit with greater magnetic coupling strength: Select a stirrer with a larger drive magnet (>12 cm in length), heavy-duty motor, and the capacity to accommodate longer stir bars.

Hazardous Environment

Organic solvents and chemical mixtures often pose a hazard in your lab because standard heating and stirring equipment can ignite fumes at medium to high temperatures. Reduce your risk of damage, injury, and increased liability by using only explosion-proof equipment.

Reference source:  http://www.coleparmer.com/TechLibraryArticle/696